AMB2018-01-15.5-CBM-B2-P1-L8-Trans-MS-EDS.xml AM-Bench-2018 (Version 1)
BenchMark Description: Laser powder bed fusion 3D builds and single scan laser traces of nickel-based superalloy IN625 and 15-5 stainless steel
Description: Laser powder bed fusion 3D builds of nickel-based superalloy IN625 and 15-5 stainless steel test objects
AMB2018-01 Description: https://www.nist.gov/ambench/amb2018-01-description
BenchMark ID: AMB2018-01-15.5-CBM-B2-P1-L8-Trans-MS-EDS
Build Number: 2
Part Number: 1
Leg Number: 8
Sample Owner MML/642-MW
Measurment Date 2018-04-23
Material
Material 15-5 PH CompositionFe-14.9Cr-4.3Ni-3.9Cu-0.5Si-0.3Nb-0.1Mn-0.02C-0.004N mass percent
Chemical Analysis: https://s3.amazonaws.com/nist-midas/1889/AMB2018-01_15-5_MaterialCertificate.pdf
Particle Distribution| PH15-5-D10 | 20.4 |
|---|---|
| PH15-5-D50 | 34.0 |
| PH15-5-D90 | 50.6 |
Build Process
Scan Description https://www.nist.gov/ambench/amb2018-01-description
Total Number of Layers 625
Layer Height in microns 20
Hatch Distance in microns 100
Laser Time off between Infill (ms) 6.70
| Laser Type | Continuous-wave ytterbium fiber |
|---|---|
| Contour Laser Power ( W ) | 100 |
| Infill Laser Power ( W ) | 195 |
| Contour Scan Speed ( mm/s ) | 900 |
| Infill Scan Speed ( mm/s ) | 800 |
| Spot Diameter ( micrometer ) | 50 |
Post Build Process
As-BuiltSEM Image
Instrument: JEOL-JSM7100
Aquisition Date: 2018-04-23
Aquisition Time: 16:34:06
Instrument Metadata:
EDS Maps
| Image Width: | 12microns |
|---|---|
| Image Height: | 8.96microns |
| Magnification: | 10000 |
| EDS Acceleratating Voltage: | 15kV |
| Working-Distance: | 10.1mm |
| StandardUse: | no x |
| Step Size: | |
| Frame Average: | |
| File: Fe K-Alpha | |
| Map Image Type: | PNG |
| Description: | |
| Map File:Fe K-Alpha | Click here to Download the image file |
| File: Cr K-Alpha1 | |
| Map Image Type: | PNG |
| Description: | |
| Map File:Cr K-Alpha1 | Click here to Download the image file |
| File: O K-Alpha 1 | |
| Map Image Type: | PNG |
| Description: | |
| Map File:O K-Alpha 1 | Click here to Download the image file |
| File: Si K-Alpha 1 | |
| Map Image Type: | PNG |
| Description: | |
| Map File:Si K-Alpha 1 | Click here to Download the image file |
| File: Mn K-Alpha1 | |
| Map Image Type: | PNG |
| Description: | |
| Map File:Mn K-Alpha1 | Click here to Download the image file |
| File: Nb K-Alpha 1 | |
| Map Image Type: | PNG |
| Description: | |
| Map File:Nb K-Alpha 1 | Click here to Download the image file |
| File: Cu K-Alpha 1,2 | |
| Map Image Type: | PNG |
| Description: | |
| Map File:Cu K-Alpha 1,2 | Click here to Download the image file |
| File: Mo L-Alpha1 | |
| Map Image Type: | PNG |
| Description: | |
| Map File:Mo L-Alpha1 | Click here to Download the image file |
| File: C K-Alpha 1,2 | |
| Map Image Type: | PNG |
| Description: | |
| Map File:C K-Alpha 1,2 | Click here to Download the image file |
| File: Ni K-Alpha 1 | |
| Map Image Type: | PNG |
| Description: | |
| Map File:Ni K-Alpha 1 | Click here to Download the image file |
| File: N K-Alpha 1,2 | |
| Map Image Type: | PNG |
| Description: | |
| Map File:N K-Alpha 1,2 | Click here to Download the image file |
| Map File: Fe Kalpha | |
| Map Image Type: | TIFF |
| Description: | Label: Fe Kα1 Collected: 4/23/2018 4:34:06 PM Resolution (Width): 4096 pixels Resolution (Height): 3072 pixels Image Width: 12μm Image Height: 8.96μm Magnification: 10000 x Binning Factor: 1 Smoothing Level: 1 Number of Completed Frames: 1 Dwell Time: 4ms Energy Range (keV): 20 keV Number Of Channels: 2048 Process Time: 3 Maximum pixel value: 27.0 counts Total Counts in Element Map: 104271889.0 counts Primary Detector: Primary Detector Serial Number: 36354-X080 |
| Map File: Fe Kalpha | Click here to Download the image file |
| Map File: Cr Kalpha1 | |
| Map Image Type: | TIFF |
| Description: | Label: Cr Kα1 Collected: 4/23/2018 4:34:06 PM Resolution (Width): 4096 pixels Resolution (Height): 3072 pixels Image Width: 12μm Image Height: 8.96μm Magnification: 10000 x Binning Factor: 1 Smoothing Level: 1 Number of Completed Frames: 1 Dwell Time: 4ms Energy Range (keV): 20 keV Number Of Channels: 2048 Process Time: 3 Maximum pixel value: 16.0 counts Total Counts in Element Map: 35592785.2 counts Primary Detector: Primary Detector Serial Number: 36354-X080 |
| Map File: Cr Kalpha1 | Click here to Download the image file |
| Map File: O Kalpha1 | |
| Map Image Type: | TIFF |
| Description: | Label: O Kα1 Collected: 4/23/2018 4:34:06 PM Resolution (Width): 4096 pixels Resolution (Height): 3072 pixels Image Width: 12μm Image Height: 8.96μm Magnification: 10000 x Binning Factor: 1 Smoothing Level: 1 Number of Completed Frames: 1 Dwell Time: 4ms Energy Range (keV): 20 keV Number Of Channels: 2048 Process Time: 3 Maximum pixel value: 9.7 counts Total Counts in Element Map: 12246456.5 counts Primary Detector: Primary Detector Serial Number: 36354-X080 |
| Map File: O Kalpha1 | Click here to Download the image file |
| Map File: Si Kalpha1 | |
| Map Image Type: | TIFF |
| Description: | Label: Si Kα1 Collected: 4/23/2018 4:34:06 PM Resolution (Width): 4096 pixels Resolution (Height): 3072 pixels Image Width: 12μm Image Height: 8.96μm Magnification: 10000 x Binning Factor: 1 Smoothing Level: 1 Number of Completed Frames: 1 Dwell Time: 4ms Energy Range (keV): 20 keV Number Of Channels: 2048 Process Time: 3 Maximum pixel value: 8.0 counts Total Counts in Element Map: 7703079.4 counts Primary Detector: Primary Detector Serial Number: 36354-X080 |
| Map File: Si Kalpha1 | Click here to Download the image file |
| Map File: Mn Kalpha1 | |
| Map Image Type: | TIFF |
| Description: | Label: Mn Kα1 Collected: 4/23/2018 4:34:06 PM Resolution (Width): 4096 pixels Resolution (Height): 3072 pixels Image Width: 12μm Image Height: 8.96μm Magnification: 10000 x Binning Factor: 1 Smoothing Level: 1 Number of Completed Frames: 1 Dwell Time: 4ms Energy Range (keV): 20 keV Number Of Channels: 2048 Process Time: 3 Maximum pixel value: 7.4 counts Total Counts in Element Map: 6805952.7 counts Primary Detector: Primary Detector Serial Number: 36354-X080 |
| Map File: Mn Kalpha1 | Click here to Download the image file |
| Map File: Nb Kalpha1 | |
| Map Image Type: | TIFF |
| Description: | Label: Nb Lα1 Collected: 4/23/2018 4:34:06 PM Resolution (Width): 4096 pixels Resolution (Height): 3072 pixels Image Width: 12μm Image Height: 8.96μm Magnification: 10000 x Binning Factor: 1 Smoothing Level: 1 Number of Completed Frames: 1 Dwell Time: 4ms Energy Range (keV): 20 keV Number Of Channels: 2048 Process Time: 3 Maximum pixel value: 8.0 counts Total Counts in Element Map: 6320016.2 counts Primary Detector: Primary Detector Serial Number: 36354-X080 |
| Map File: Nb Kalpha1 | Click here to Download the image file |
| Map File: Cu Lalpha1,2 | |
| Map Image Type: | TIFF |
| Description: | Label: Cu Lα1,2 Collected: 4/23/2018 4:34:06 PM Resolution (Width): 4096 pixels Resolution (Height): 3072 pixels Image Width: 12μm Image Height: 8.96μm Magnification: 10000 x Binning Factor: 1 Smoothing Level: 1 Number of Completed Frames: 1 Dwell Time: 4ms Energy Range (keV): 20 keV Number Of Channels: 2048 Process Time: 3 Maximum pixel value: 8.0 counts Total Counts in Element Map: 6229081.9 counts Primary Detector: Primary Detector Serial Number: 36354-X080 |
| Map File: Cu Lalpha1,2 | Click here to Download the image file |
| Map File: Mo Lalpha1 | |
| Map Image Type: | TIFF |
| Description: | Label: Mo Lα1 Collected: 4/23/2018 4:34:06 PM Resolution (Width): 4096 pixels Resolution (Height): 3072 pixels Image Width: 12μm Image Height: 8.96μm Magnification: 10000 x Binning Factor: 1 Smoothing Level: 1 Number of Completed Frames: 1 Dwell Time: 4ms Energy Range (keV): 20 keV Number Of Channels: 2048 Process Time: 3 Maximum pixel value: 8.0 counts Total Counts in Element Map: 6090369.4 counts Primary Detector: Primary Detector Serial Number: 36354-X080 |
| Map File: Mo Lalpha1 | Click here to Download the image file |
| Map File: C Kalpha1_2 | |
| Map Image Type: | TIFF |
| Description: | Label: C Kα1_2 Collected: 4/23/2018 4:34:06 PM Resolution (Width): 4096 pixels Resolution (Height): 3072 pixels Image Width: 12μm Image Height: 8.96μm Magnification: 10000 x Binning Factor: 1 Smoothing Level: 1 Number of Completed Frames: 1 Dwell Time: 4ms Energy Range (keV): 20 keV Number Of Channels: 2048 Process Time: 3 Maximum pixel value: 7.0 counts Total Counts in Element Map: 5693764.7 counts Primary Detector: Primary Detector Serial Number: 36354-X080 |
| Map File: C Kalpha1_2 | Click here to Download the image file |
| Map File: Ni Kalpha1 | |
| Map Image Type: | TIFF |
| Description: | Label: Ni Kα1 Collected: 4/23/2018 4:34:06 PM Resolution (Width): 4096 pixels Resolution (Height): 3072 pixels Image Width: 12μm Image Height: 8.96μm Magnification: 10000 x Binning Factor: 1 Smoothing Level: 1 Number of Completed Frames: 1 Dwell Time: 4ms Energy Range (keV): 20 keV Number Of Channels: 2048 Process Time: 3 Maximum pixel value: 7.0 counts Total Counts in Element Map: 5270509.4 counts Primary Detector: Primary Detector Serial Number: 36354-X080 |
| Map File: Ni Kalpha1 | Click here to Download the image file |
| Map File: N Kalpha1_2 | |
| Map Image Type: | TIFF |
| Description: | Label: N Kα1_2 Collected: 4/23/2018 4:34:06 PM Resolution (Width): 4096 pixels Resolution (Height): 3072 pixels Image Width: 12μm Image Height: 8.96μm Magnification: 10000 x Binning Factor: 1 Smoothing Level: 1 Number of Completed Frames: 1 Dwell Time: 4ms Energy Range (keV): 20 keV Number Of Channels: 2048 Process Time: 3 Maximum pixel value: 6.0 counts Total Counts in Element Map: 2609223.8 counts Primary Detector: Primary Detector Serial Number: 36354-X080 |
| Map File: N Kalpha1_2 | Click here to Download the image file |
| Support File: 15-5_CBM_B2_P1_L8 blue thin_042318_Map Details.txt | |
| File Type: | text |
| Description: | Map details |
| Result file: | Click here to Download the image file |
| Support File: 15-5_CBM_B2_P1_L8 blue thin_042318_Map Sum Spectrum.txt | |
| File Type: | text |
| Description: | Map Spectrum |
| Result file: | Click here to Download the image file |
| Support File: 15-5_CBM_B2_P1_L8 blue thin_042318_Fe_KA_Scale Bar.tiff | |
| File Type: | TIFF |
| Description: | Scale bar |
| Result file: | Click here to Download the image file |
| Support File: 15-5_CBM_B2_P1_L8 blue thin_042318_pre map Electron Image.tiff | |
| File Type: | TIFF |
| Description: | SE Image before mapping |
| Result file: | Click here to Download the image file |
| Support File: 15-5_CBM_B2_P1_L8 blue thin_042318_post map Electron Image.tiff | |
| File Type: | TIFF |
| Description: | SE Image after mapping |
| Result file: | Click here to Download the image file |
